To find chemical equilibrium, the following chemical equation is used in the experiment: Fe3+(aq) + SCN-(aq) FeSCN2+(aq). When iron (III) and thiocyanate react, thiocyanoiron (III) is produced. When the concentration of all ions at equilibrium are known, the equilibrium constant can be calculated by dividing the equilibrium concentration of the reactant by the equilibrium concentration of the products. In this experiment, four equilibrium systems containing different concentrations of three different ion types (Fe(NO3)3, KSCN-, and distilled water) are made and used to determine equilibrium concentrations. The equilibrium concentrations are used to calculate the concentration that all of the components of the chemical equation are at equilibrium. Using a colorimeter or spectrometer to determine the equilibrium concentration of FeSCN2+(aq) and …show more content…
Prepare the standard solution of FeSCN2+ pipetting 18 mL of 0.200 M Fe(NO3)3 in a 20 * 150 mm test tube labeled five. Pipet 2 mL 0.0020 M KSCN into the test tube and stir. 6. Prepare a blank. Fill the plastic cuvette ¾ full with distilled H2O. Properly clean the cuvette and handle only by the top ribbed edge while wearing gloves. Dislodge any bubbles by tapping on a hard surface and position the cuvette in the spectrometer so light passes through the clear side. 7. Connect the spectrometer to Labquest and select a new file. Calibrate the spectrometer by placing the blank inside and allowing the lamp to warm up. The optimal wavelength for the standard curve and data collection can be started at this stage. Empty the blank and use the solution from test tube one to rinse the cuvette twice. Fill it ¾ with solution one, wipe the outside, and place it in the spectrometer. 8. Start data collection and display a full spectrum graph. Stop the data and the wavelength of maximum absorbance will be identified. Under the Meter tab, select mode and then events with entry. Type in the name as concentration and the units as
While the solution dissolved, 50 mL of distilled water was added to a 150 mL beaker and heated on the hot plate. When the solution started to boil 2.65 grams of Na2SiO3*5H2O was added to the beaker with a stir bar and heated to a gentle boil. When both solutions began to boil, the sodium silicate solution was slowly added to the sodium aluminate. The solution was kept at 900C for 60 minutes and stirred with stir bar. After 60 minutes, the zeolite solution was cooled for 5 minutes and for the magnetized zeolite , 0.78 grams of FeCl3 and 0.39 grams of FeSO4*7H2O was added to the flask and stirred until the iron parts dissolved.
2. Add 8cm³ of sodium carbonate to each tube using a measuring cylinder. 3. Measure out the strontium nitrate for each boiling tube and add it (boiling tube 1 contains 1cm³, test tube 2 contains 2cm³ and so on). 4.
The cuvette was placed in the spectrophotometer with the arrows, on both the cuvette and the SpectroVis, facing the same side. After the recording, the cuvette was removed from the SpectroVis and the content was poured back into the original volumetric flask. The absorbance as well as the maximum wavelength of each solution was recorded in Table 3 and
These difficulties might have caused me to make mistakes on the amount needed to pipette or the type of substance. Overall, next time I would have made sure to pay closer attention to the pipetting portion of the procedure. Furthermore, we could extend this experiment by trying different kinds of
A. Hold the grating several inches from your face, at an angle. Look at the grating that you will be using. Record what details you see at the grating surface. I see the different colors of the rainbow when holding the grating several inches from my face.
Mika Nijhawan 9/29- 10/10 2 MENTOS AND SODA LAB REPORT State the Problem Does the type of soda affect the size of the explosion, after mentos are added? Develop a Hypothesis If seven mentos to a 2L bottle of Diet Pepsi, then it will create the biggest geyser out of Coke, Fanta, & Root Beer because Diet Pepsi has potassium benzoate, aspartame, and the carbonation which react to mentos. Design an Experiment Materials List: 1 clear test tube 35 original flavored Mentos candies (2 1/2 rolls) 1 3x5 index card 4 2L bottles of soda (all different flavors/types) 1 2L bottle of soda water 1 100 mL graduated cylinder 1 400 mL beaker 1 pair of tweezers (preferably large) 1 small container Procedure: Stack seven mentos in the test tube When given permission take the test tube, soda bottles, index cards, and the remaining 25 mentos, to the designated area Place one of the four soda bottles on a flat area Open the soda bottle and place the 3x5 index card over it With the index card over the soda bottle, flip the test tube over and place it on the index card, so the test tube is lined with
Fill each cuvettes with its respective solution. Turn on the spectrophotometer, so it can warm up then calibrate it to 0% absorbance. Put the corresponding extract blank and set the spectrophotometer to 100% transmittance, then calibrate it to 540 nm. Once catechol is added in the cuvettes, make sure the solution is mixed. Place carrot cuvette in the spectrophotometer and record the resulting transmittance.
Step 2: Mix both test tubes , shake gently and time the reaction. Step 3: The same step as procedure 1, and step 3 which is to record the observed color step 4: use the palette/color chart to help you identify the observations you make. Safety precautions: Pull your hair back Safety eye goggles Closed toe
Data for determining the concentration of the unknown ferricyanide solution Peak Current (A) Calibration Line Cathodic 3.00E-5 y = 6.00E-6x 1.00E-6 Anodic 2.15E-5 y = 5.00E-6x
The colorimeter must be set to the correct wavelength setting. In this experiment, the wavelength must be set to blue so it can
11) After you have prepared the dilutions, clean the outsides of the cuvettes with a paper towel. 12) Place the blank tube (tube 0) in the spectrophotometer. Since distilled water has no color it will not absorb any light so the absorbance number would be zero and this done to test the absorbance scale on the Spectrophotometer for the purpose of having it calibrated correctly. 13) Set the spectrometer to a wavelength of 530 nanometers. 14) Place the cuvettes (numbers 1-6) with the appropriate substance and record it’s reading in the data table.
The tube “B” had only water in it so it was acting as our blank, a blank in our experiment was used to calibrate the spectrophotometer machine, it was identical to other tubes only that it did not have the solute that we were
Research question What is the effect of temperature Amylase activity? Word count-1453 Background research Enzymes are biological catalysts that speed up a chemical reactions. They do this by decreasing the activation energy(the energy needed to start the reaction) of a chemical reaction. The enzyme present in our saliva is called Amylase. Amylase increases the rate of reaction by decreasing the activation energy needed to hydrolyse the starch molecules.
We started the experiment with part 1 of the lab using 0.20 M to find a standard absorbance curve for [FeSCN2+], we found the max absorbance which we would use would be at 432.6nm. Once we had this absorbance, we used that data to create our absorbance vs. concentration graph which was 3635x + 0.0449, with an r2. After this we did part 2 of the lab, where we got 5 different test tubes to measure the absorbance with varying amounts of 0.002 M Fe(NO3)3 and 0.002 M SCN- and H2O, and we subtracted the absorbance of test tubes 1-4 from the absorbance of test tube 1 to get the net absorbance. After this we plugged in the net absorbance from part 2 to the equation from part 1, this result gave us the concentration at equilibrium, so that we could
Introduction: The objective for the lab was to determine properties of materials by using a tension test. The properties that were determined was Young’s Modulus, ultimate tensile strength, and yield strength. Three aluminum alloys were tested. The first was the AA 2024 , which is high strength used in aerospace applications.