ipl-logo

Nmr Spectroscopy Lab Report

1580 Words7 Pages

Introduction of NMR spectroscopy Nuclear Magnetic Resonance (NMR) spectroscopy is a form of absorption spectroscopy by which a nuclei under investigation absorbs the energy from an external magnetic field and resonances or excites from a low energy state to a high energy state. It involves the disintegration of spin state into two spin states of unequal energy. The emerging radiofrequency is absorbed in a magnetic field resulting to the magnetic properties of the nuclei which getting up from the axial spin. Hence, different NMR absorption spectrum can be obtained which contains one to several groups of absorption lines in the radiofrequency part of the electromagnetic spectrum depends on the particular nucleus. Apparently, the location of peaks …show more content…

For the frequency sweep method, the precession frequency is permanent if the applied magnetic field is unchanged and the frequency of the radiofrequency field must be changed for resonance. Therefore, resonance is achieved by keeping the applied magnetic field constant and scanning the radiofrequency transmitter through the continuous variation in oscillating frequency. On the other hand, the field sweep method is achieved by continuous variation in the magnetic field but keeping the oscillating frequency constant. Among the two sweep methods, field sweep method is the most common method utilized in NMR. This is because of the ease of changing the magnetic field than the radiofrequency radiation in order to bring about resonance in nuclei. [3] 5. Radiofrequency transmitter It is used to generate the radiofrequency radiation which is needed to induce transition in the nuclei of the sample from the lower energy state to the higher energy state. It is attached at the right angles to the path of the field around the sample probe which is perpendicular to the magnetic field in order to achieve the maximum interaction with the sample. The oscillator then irradiates the sample with radiofrequency radiation and transmits radio waves of fixed frequency such as 60, 100, 200 or 300 MHz to a small coil that drives the sample in the probe. [3] 6. Radiofrequency

Show More
Related
202 Words | 1 Pages

C4564 Description: IC50: 3-AP is a ribonucleotide reductase inhibitor and iron chelator with antitumor activity. Ribonucleotide reductase, the rate-limiting enzyme for de novo DNA synthesis, is an excellent target for chemotherapy. Its increased activity in cancer cells is associated with malignant transformation and proliferation.

Read More
638 Words | 3 Pages

For most sequences at position 4 and 5 we observe only the nucleotides G and T, respectively. There may be rare cases where other nucleotides may also be found. To consider such observations, we need to do a process called additive smoothing or Laplace smoothing to smooth the categorical data. [9] In this case, we add 4 sequences: AAAAAAAAA, CCCCCCCCC, GGGGGGGG, TTTTTTTTT.

Read More
310 Words | 2 Pages

I need to find the area of rectangle ABCD. I know that ABCD is a rectangle with diagonals intersecting at point E. Segment DE equals 4x-5, segment BC equals 2x+6, and segment AC equals 6x. I predict that To find the area of rectangle ABCD I need to find out the base and height of the rectangle. The first step is to find what x equals. Since I know the intersecting line segments AC and DB are congruent that means when I times the equation 4x-5 for segment DE by two it will equal the equation 6x for segment AC.

Read More
247 Words | 1 Pages

1. The test subjects will prepare for sleep by acquiring everything needed for the subjects’ sleep preferences. 2. The test subjects will all set alarms on their smartphones for approximately 6, 8, and 10 hours after the subjects’ enter the resting period (Subjects may wake during the resting period for the bathroom, but they must not stay awake for more than ten minutes at a time to prevent as much deviation as possible.). 3.

Read More
265 Words | 2 Pages

\section{Facility Static and Dynamic Control}\label{Calibr} The facility calibration is the transfer function between the oscillating gauge pressure $P_C(t)$ in the chamber (described in ~\autoref{Sub31}) and the liquid flow rate $q(t)$ in the distributing channel, i.e. the test section. Due to practical difficulties in measuring $q(t)$ within the thin channel, and being the flow laminar, this transfer function was derived analytically and validated numerically as reported in ~\autoref{Sub32} and ~\autoref{Sub33}. \subsection{Pressure Chamber Response}\label{Sub31} Fig.\ref{fig:2a} shows three example of pressure signals $P_C(t)$, measured in the pneumatic chamber.

Read More
151 Words | 1 Pages

Equipment list: 1. Agilent 54621A oscilloscope 2. Agilent 33120 Function Generator 3. Capacitors 4.

Read More
574 Words | 3 Pages

Experiment 7 In this experiment we configured several DC circuits consisting of an emf and a network of resistors. The circuits were composed of a power supply, two DMMs, a circuit board, an SPST switch, and an assortment of known resistors along with one unknown resistor. We measured the current and voltage of the entire circuit as well as the potential drops across each resistor to determine the parameters of the circuit including the resistance, voltage, and current for each component.

Read More
333 Words | 2 Pages

Using the data provided in each one of these tests it can be assumed that one has done the steps to be able to determine the magnitude and orientation of the charges of the tape in each test, thus, allowing them to apply the same principle to any object they so desired. Their results would line up with the following; that if the two pieces of tape are torn from the same 40 centimeter strip then the tops of both pieces of tape would be positive and the bottoms of both pieces of tape would be negative and that if they would double the tape the attraction or repulsion in general would lower due to the increased density. Their data would also show that two pieces of tape ripped from each other would result in one piece being entirely positive and the other being entirely negative, they would also be able to state that the orientation of how the tape is paired up doesn’t matter.

Read More
1392 Words | 6 Pages

1. Identify the range of senses involved in communication • Sight (visual communication), Touch (tactile communication), Taste, Hearing (auditory communication), Smell (olfactory communication) 2. Identify the limited range of wavelengths and named parts of the electromagnetic spectrum detected by humans and compare this range with those of THREE other named vertebrates and TWO named invertebrates. Figure 1: the electromagnetic spectrum source: www.ces.fau.edu Vertebrates Human Japanese Dace Fish Rattlesnake Zebra Finch Part of electromagnetic spectrum detected ROYGBV (visible light) detected by light sensitive cells in the eye called rods and cones.

Read More
362 Words | 2 Pages

1. There are two ways of maximizing points in this experiment. The first one is that I should connect myself to a vertex that is in the biggest component and purchases immunization. Since the probability of being infected is based off of expected value, I would have less than 1% chance of getting infected. The second way is that I try to make myself stay in the second-largest connected component.

Read More
407 Words | 2 Pages

• Write down the highlighted numbers. Do you observe a pattern? • Does the pattern grow? What is the reason for this? • Write down the last number (say 53).

Read More
596 Words | 3 Pages

Figure shows the intersection of line joining the camera center and image points ${\bf x}$ and ${\bf x'}$ which will be the 3D point ${\bf X}$.\\ \end{figure} The ‘gold standard’ reconstruction algorithm minimizes the sum of squared errors between the measured and predicted image positions of the 3D point in all views in which it is visible, i.e.\\ \begin{equation} {\bf X=\textrm{arg min} \sum_{i} ||x_i-\hat{x_i}(P_i,X)||^2} \end{equation} Where ${\bf x_i}$ and ${\bf \hat{x_i}(P_i,X)}$ are the measured and predicted image positions in view $i$ under the assumption that image coordinate measurement noise is Gaussian-distributed, this approach gives the maximum likelihood solution for ${\bf X}$. Hartley and Sturm [3] describe a non-iterative

Read More
173 Words | 1 Pages

(a) 3Mbps / 150Kbpa =3 X 1024 / 150 = 3072 / 150 =20.48 20 Users can be supported 150Kbps dedicated. (b)

Read More
313 Words | 2 Pages

Elijah Brycth B. Jarlos IX-Argon 1. Multicellularity is a condition of an organism to have multicellular cells. An example of a organism who has multicellular cells are plants, animals, and humans. The main reason of why scientists have a hard time finding a good set of existing organisms to compare. Is neither the first set of organisms which is being compared is dying as fast as the second specimen is being examined or they just can’t find the right species.

Read More
1486 Words | 6 Pages

Introduction The purpose of this lab is to use control variables to help identify different macromolecules. Biological systems are made up of these four major macromolecules: carbohydrates, lipids, proteins and nucleic acids. Carbohydrates are sugar molecules (monosaccharides, disaccharides, and polysaccharides) which make them the most abundant macromolecule on the earth. Lipids (oils and fats, phospholipids and steroids) are insoluble in water and perform many functions such as energy source, essential nutrients, hormones and insulators (Lehman, 1955).

Read More

More about Nmr Spectroscopy Lab Report

Open Document